ADBB

CAS No.
Chemical Name:
adbb
Synonyms
adbb;ADB-BUTINACA
CBNumber:
CB74858123
Molecular Formula:
Formula Weight:
0

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ADBB

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CAS No.
Chemical Name:
adbb
Synonyms
adbb;ADB-BUTINACA
CBNumber:
CB74858123
Molecular Formula:
Formula Weight:
0
SKU: N/A Category:

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Description

Structure

A solution of ethyl methyl amine (10Og, 1.69mol) in dichloromethane (1.51) is added dropwise to a slurry of sodium bicarbonate (284g, 3.384mol) and triphosgene (332g, 1.117mol) in dichloromethane (21) at 10-15°C over 2 hours. The reaction mixture is stirred at room temperature for 3 hours. The reaction mass is filtered to remove sodium chloride and the filtrate is concentrated under vacuum to give 189g of ethyl methyl carbamoyl chloride as a light yellow oil (yield: 92percent). The process of was repeated but the solvent was changed to dichloromethane. The other conditions were similar. The results are provided in Table 2 below.Table 2The yield was found to be consistent a

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100 grams, 25 grams, 250 grams, 50 grams, 500 grams

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Structure

A solution of ethyl methyl amine (10Og, 1.69mol) in dichloromethane (1.51) is added dropwise to a slurry of sodium bicarbonate (284g, 3.384mol) and triphosgene (332g, 1.117mol) in dichloromethane (21) at 10-15°C over 2 hours. The reaction mixture is stirred at room temperature for 3 hours. The reaction mass is filtered to remove sodium chloride and the filtrate is concentrated under vacuum to give 189g of ethyl methyl carbamoyl chloride as a light yellow oil (yield: 92percent). The process of was repeated but the solvent was changed to dichloromethane. The other conditions were similar. The results are provided in Table 2 below.Table 2The yield was found to be consistent a

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